3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt

Base Information

Chemical Name:3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt
CAS No.:1467663-56-4
Molecular Formula:C₇H₆O₂*C₁₂H₂₃NO₂S
Molecular Weight:367.51
Hs Code.:

Synonyms:

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Chemical Property of 3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt

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Technology Process of 3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt

There total 3 articles about 3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine

: 65-85-0,8013-63-6
benzoic acid

: 1467663-56-4
3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt

Guidance literature:: In toluene; for 18h;

Reference yield:

: 41353-91-7
1’-azaspiro[oxirane-2,3’-bicyclo[2.2.2]octane]

: 1467663-56-4
3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / toluene; methanol / 1.5 h / 0 - 20 °C

2: toluene / 18 h

With potassium tert-butylate; In methanol; toluene;

Reference yield:

: 1193-65-3
3-quinuclidinone hydrochloride

: 1467663-56-4
3-hydroxy-3-[(1-ethoxyethyl)mercaptomethyl]quinuclidine benzoic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / dimethyl sulfoxide / 16.75 h / 0 - 20 °C / Inert atmosphere

2: potassium tert-butylate / toluene; methanol / 1.5 h / 0 - 20 °C

3: toluene / 18 h

With potassium tert-butylate; In methanol; dimethyl sulfoxide; toluene;