C₃₁H₃₆⁽²⁾HNO₇Si

Base Information

Chemical Name:C₃₁H₃₆⁽²⁾HNO₇Si
CAS No.:1562377-44-9
Molecular Formula:C₃₁H₃₇NO₇Si
Molecular Weight:564.715
Hs Code.:

C<sub>31</sub>H<sub>36</sub><sup>(2)</sup>HNO<sub>7</sub>Si

Synonyms:

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Chemical Property of C₃₁H₃₆⁽²⁾HNO₇Si

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Technology Process of C₃₁H₃₆⁽²⁾HNO₇Si

There total 6 articles about C₃₁H₃₆⁽²⁾HNO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1562377-15-4
C₂₉H₃₉NO₃Si

: 1562377-44-9
C₃₁H₃₆⁽²⁾HNO₇Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetradeuterioacetic acid / Inert atmosphere

2.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran / 0.17 h / -78 °C / Molecular sieve; Inert atmosphere

2.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

3.1: benzene / 150 °C / Sealed tube; Inert atmosphere

With n-butyllithium; tetradeuterioacetic acid; potassium tert-butylate; In tetrahydrofuran; benzene;
DOI:10.1021/ol4034447

Reference yield:

: 889-31-6
5,5-dimethyl-3-benzylamino-2-cyclohexen-1-one

: 1562377-44-9
C₃₁H₃₆⁽²⁾HNO₇Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Molecular sieve; Inert atmosphere

1.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran / 5 h / 0 °C / Molecular sieve; Inert atmosphere

2.2: 2 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

3.1: tetradeuterioacetic acid / Inert atmosphere

4.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran / 0.17 h / -78 °C / Molecular sieve; Inert atmosphere

4.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

5.1: benzene / 150 °C / Sealed tube; Inert atmosphere

With n-butyllithium; tetradeuterioacetic acid; potassium tert-butylate; potassium hexamethylsilazane; In tetrahydrofuran; benzene;
DOI:10.1021/ol4034447

Reference yield:

: 1562377-09-6
C₂₃H₂₅NO₃

: 1562377-44-9
C₃₁H₃₆⁽²⁾HNO₇Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 5 h / 0 °C / Molecular sieve; Inert atmosphere

1.2: 2 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

2.1: tetradeuterioacetic acid / Inert atmosphere

3.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran / 0.17 h / -78 °C / Molecular sieve; Inert atmosphere

3.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

4.1: benzene / 150 °C / Sealed tube; Inert atmosphere

With n-butyllithium; tetradeuterioacetic acid; potassium tert-butylate; potassium hexamethylsilazane; In tetrahydrofuran; benzene;
DOI:10.1021/ol4034447