C₁₁H₁₃N*ClH

Base Information

Chemical Name:C₁₁H₁₃N*ClH
CAS No.:153396-15-7
Molecular Formula:C₁₁H₁₃N*ClH
Molecular Weight:195.692
Hs Code.:

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Suppliers and Price of C₁₁H₁₃N*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₃N*ClH

Chemical Property:

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Technology Process of C₁₁H₁₃N*ClH

There total 1 articles about C₁₁H₁₃N*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1407998-83-7
2-(1-phenylpent-1-yn-3-yl)isoindoline-1,3-dione

: 153396-15-7
C₁₁H₁₃N*ClH

Guidance literature:: 2-(1-phenylpent-1-yn-3-yl)isoindoline-1,3-dione; With hydrazine hydrate; at 45 ℃;

With hydrogenchloride; In ethanol; at 20 ℃; for 0.25h;
DOI:10.1002/anie.201402614

Reference yield: 89.0%

: 153396-15-7
C₁₁H₁₃N*ClH

: 25895-60-7
sodium cyanoborohydride

: 1610970-34-7
C₁₂H₁₅BN₂

Guidance literature:: With magnesium sulfate; In tetrahydrofuran; for 24h; Reflux;
DOI:10.1002/anie.201402614

Reference yield:

: 153396-15-7
C₁₁H₁₃N*ClH

: 1610970-49-4
C₁₂H₁₅BN₂

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate / tetrahydrofuran / 24 h / Reflux

2: XPhosAu(triazole)OTf / 1,2-dichloro-ethane / 72 h / 80 °C

With XPhosAu(triazole)OTf; magnesium sulfate; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1002/anie.201402614