C₄₅H₃₀ClIrN₄O

Base Information

Chemical Name:C₄₅H₃₀ClIrN₄O
CAS No.:109432-33-9
Molecular Formula:C₄₅H₃₀ClIrN₄O
Molecular Weight:870.432
Hs Code.:

C<sub>45</sub>H<sub>30</sub>ClIrN<sub>4</sub>O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₃₀ClIrN₄O

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Technology Process of C₄₅H₃₀ClIrN₄O

There total 4 articles about C₄₅H₃₀ClIrN₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 80937-33-3
oxygen

: 917-23-7,20998-75-8
5,15,10,20-tetraphenylporphyrin

: 109432-33-9
C₄₅H₃₀ClIrN₄O

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; for 96h; Reflux;
DOI:10.1039/c4cc02759k

Reference yield: 25.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 34135-21-2
2Ir⁽¹⁺⁾*6CO*2Cl^(1-)={Ir(CO)3Cl}2

: 114763-61-0
((C₆H₅)4C₂₀H₈N₄)^(2-)*2Ir⁽¹⁺⁾*6CO=((C₆H₅)4C₂₀H₈N₄){Ir(CO)3}2

: 109432-33-9
{chlorocarbonyl(5,10,15,20-tetraphenylporphyrin)iridium}

Guidance literature:: In methanol; benzene; stirring at 35°C for 10 h, protected from light; filtn., evapn., sepn. on silica gel: first eluate is (TPP)H2, followed by (TPP)Ir(CO)(Cl) and (TPP)(Ir(CO)3)2; this is further purified on silica gel, followed by recrystn. from CH2Cl2/hexane;