bis(2,6-difluorophenyl)mercury

Base Information

Chemical Name:bis(2,6-difluorophenyl)mercury
CAS No.:80006-60-6
Molecular Formula:C₁₂H₆F₄Hg
Molecular Weight:426.763
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2,6-difluorophenyl)mercury

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Technology Process of bis(2,6-difluorophenyl)mercury

There total 4 articles about bis(2,6-difluorophenyl)mercury which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.3%

: 7783-39-3
mercury(II) fluoride

: 133117-48-3
1,3-difluoro-2-trimethylsilylbenzene

: 80006-60-6
bis(2,6-difluorophenyl)mercury

Guidance literature:: In dimethyl sulfoxide; byproducts: (CH3)3SiF; HgF2 suspended in DMSO in a Schlenk-tube and (CH3)3SiC6H3F2 added to this soln. at room temp.; reacted for 48-72 h; solid precipitate filtered and washed with DMSO; filtrate and washing liquid added to water; precipitate collected by filtration and dried over concentrated H2SO4;
DOI:10.1002/zaac.200400244

Reference yield: 49.0%

: mercury(II) 2,6-difluorobenzoate

: 80006-60-6
bis(2,6-difluorophenyl)mercury

: 2,6-difluorophenylmercury(II) 2,6-difluorobenzoate

Guidance literature:: In pyridine; byproducts: CO2; refluxing under N2, 20h; evapn.; extn. (warm petrol); evapn.; extn. (diethyl ether); evapn.; recrystn. (diethyl ether); elem. anal.;

Reference yield: 40.0%

: (F₂C₆H₃COO)2Hg

: 80006-60-6
bis(2,6-difluorophenyl)mercury

Guidance literature:: In dimethyl sulfoxide; reflux under N2 for 2 h; recrystn. from ethanol, and benzene/petrol, elem. anal.;
DOI:10.1016/S0022-328X(00)80993-6