Technology Process of C12H18O5S
There total 3 articles about C12H18O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
magnesium bis(monoperoxyphthalate) hexahydrate;
In
methanol;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1021/jo101877r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium methylate / N,N-dimethyl-formamide / 12 h / 20 °C
2.1: N,N,N',N'-tetramethylguanidine / N,N-dimethyl-formamide / 0.5 h / 90 °C / Inert atmosphere
2.2: 5 h / 90 °C / Inert atmosphere
3.1: magnesium bis(monoperoxyphthalate) hexahydrate / methanol / 6 h / 20 °C / Inert atmosphere
With
sodium methylate; magnesium bis(monoperoxyphthalate) hexahydrate; N,N,N',N'-tetramethylguanidine;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo101877r
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N,N',N'-tetramethylguanidine / N,N-dimethyl-formamide / 0.5 h / 90 °C / Inert atmosphere
1.2: 5 h / 90 °C / Inert atmosphere
2.1: magnesium bis(monoperoxyphthalate) hexahydrate / methanol / 6 h / 20 °C / Inert atmosphere
With
magnesium bis(monoperoxyphthalate) hexahydrate; N,N,N',N'-tetramethylguanidine;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo101877r