4-bromophenyl piperidine-1-carbodithioate

Base Information

Chemical Name:4-bromophenyl piperidine-1-carbodithioate
CAS No.:91720-56-8
Molecular Formula:C₁₂H₁₄BrNS₂
Molecular Weight:316.286
Hs Code.:

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Chemical Property of 4-bromophenyl piperidine-1-carbodithioate

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Technology Process of 4-bromophenyl piperidine-1-carbodithioate

There total 3 articles about 4-bromophenyl piperidine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 110-89-4
piperidine

: 75-15-0,12122-00-8
carbon disulfide

: 139139-81-4
bis(4-bromophenyl)iodonium triflate

: 91720-56-8
4-bromophenyl piperidine-1-carbodithioate

Guidance literature:: piperidine; carbon disulfide; In dichloromethane; at 20 ℃; for 0.0833333h; Sealed tube;

bis(4-bromophenyl)iodonium triflate; In dichloromethane; at 20 ℃; for 2h; Sealed tube;
DOI:10.1021/acs.orglett.1c02220

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 91720-56-8
4-bromophenyl piperidine-1-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 - 20 °C

2.1: dichloromethane / 0.08 h / 20 °C / Sealed tube

2.2: 2 h / 20 °C / Sealed tube

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/acs.orglett.1c02220