methyl trans-3,4-diphenylcyclopentanecarboxylate

Base Information

Chemical Name:methyl trans-3,4-diphenylcyclopentanecarboxylate
CAS No.:125250-84-2
Molecular Formula:C₁₉H₂₀O₂
Molecular Weight:280.367
Hs Code.:

Synonyms:

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Chemical Property of methyl trans-3,4-diphenylcyclopentanecarboxylate

Chemical Property:

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Technology Process of methyl trans-3,4-diphenylcyclopentanecarboxylate

There total 5 articles about methyl trans-3,4-diphenylcyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-36-6
ethyl 3-phenyl-2-propenoate

: 125250-84-2
methyl trans-3,4-diphenylcyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium / diethyl ether / 3 h / Heating

2: 20percent HBr / aq. ethanol / Heating

3: 92 percent / Zn dust, TiCl₄ / tetrahydrofuran / 2.5 h / Ambient temperature

4: 1.) BH₃*THF, 2.) 3 N NaOH, 30percent H₂O₂ / 1.) THF, 0 deg C to room temperature, 2.) room temperature, 1 h

5: 95 percent / oxalyl chloride, DMSO / CH₂Cl₂ / 0.33 h / -60 °C

6: Br₂, sodium bicarbonate buffer / H₂O

With sodium hydroxide; borane-THF; oxalyl dichloride; sodium bicarbonate buffer; hydrogen bromide; dihydrogen peroxide; bromine; sodium; titanium tetrachloride; dimethyl sulfoxide; zinc; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/jo00294a016

Reference yield:

: 7356-94-7
2,3-Diphenyl-5-oxo-cyclopentancarbonsaeureethylester

: 125250-84-2
methyl trans-3,4-diphenylcyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 20percent HBr / aq. ethanol / Heating

2: 92 percent / Zn dust, TiCl₄ / tetrahydrofuran / 2.5 h / Ambient temperature

3: 1.) BH₃*THF, 2.) 3 N NaOH, 30percent H₂O₂ / 1.) THF, 0 deg C to room temperature, 2.) room temperature, 1 h

4: 95 percent / oxalyl chloride, DMSO / CH₂Cl₂ / 0.33 h / -60 °C

5: Br₂, sodium bicarbonate buffer / H₂O

With sodium hydroxide; borane-THF; oxalyl dichloride; sodium bicarbonate buffer; hydrogen bromide; dihydrogen peroxide; bromine; titanium tetrachloride; dimethyl sulfoxide; zinc; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jo00294a016

Reference yield:

: 13351-28-5
trans-3,4-diphenylcyclopentanone

: 125250-84-2
methyl trans-3,4-diphenylcyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / Zn dust, TiCl₄ / tetrahydrofuran / 2.5 h / Ambient temperature

2: 1.) BH₃*THF, 2.) 3 N NaOH, 30percent H₂O₂ / 1.) THF, 0 deg C to room temperature, 2.) room temperature, 1 h

3: 95 percent / oxalyl chloride, DMSO / CH₂Cl₂ / 0.33 h / -60 °C

4: Br₂, sodium bicarbonate buffer / H₂O

With sodium hydroxide; borane-THF; oxalyl dichloride; sodium bicarbonate buffer; dihydrogen peroxide; bromine; titanium tetrachloride; dimethyl sulfoxide; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo00294a016