copper(II)(o-benzoylsalicylato)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate

Base Information

• Chemical Name: copper(II)(o-benzoylsalicylato)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate
• CAS No.: 277314-03-1
• Molecular Formula: C₂₄H₃₄CuN₃O₄*ClO₄
• Molecular Weight: 591.548
• Mol file: 277314-03-1.mol

Synonyms:

Chemical Property of copper(II)(o-benzoylsalicylato)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of copper(II)(o-benzoylsalicylato)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate

There total 3 articles about copper(II)(o-benzoylsalicylato)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

copper(II)(flavonolate)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate (277314-01-9) + oxygen (80937-33-3) → copper(II)(o-benzoylsalicylato)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate (277314-03-1)

Guidance literature:

In N,N-dimethyl-formamide; under Ar; Cu complex treated with dioxygen (0.1 MPa) at 100°C for8 h; cooled to room temp., diethyl ether layered on top of soln.; Kinetics;

DOI:10.1016/S1381-1169(03)00456-4

Reference yield: 62.0%

[Cu(fla)(idpaH)]ClO4 (277314-01-9) + oxygen (80937-33-3) → [Cu(idpaH)(o-bs)]ClO4 (277314-03-1)

Guidance literature:

In N,N-dimethyl-formamide; in O2 atmosphere at 100 °C stirred for 8 hs, cooled to room temp., diethyl ether layered on the soln.; pttn.; Kinetics;

DOI:10.1016/S0020-1693(00)00071-2

Reference yield: 62.0%

[Cu(flavonolate)(3,3'-iminobis(N,N-dimethylpropylamine))]ClO4 (277314-01-9) + oxygen (80937-33-3) → [Cu(3,3'-iminobis(N,N-dimethylpropylamine))(O-benzoylsalicylate)]ClO4 (277314-03-1)

Guidance literature:

In N,N-dimethyl-formamide; Cu-complex in DMF was treated with O2 0.1 MPa at 100°C for 8 h, cooled to room temp.; Et2O was layered; Kinetics;

DOI:10.1016/S0020-1693(01)00469-8

upstream raw materials:

[Cu(fla)(idpaH)]ClO₄

oxygen

[Cu(flavonolate)(3,3'-iminobis(N,N-dimethylpropylamine))]ClO₄

copper(II)(flavonolate)[3,3'-iminobis(N,N-dimethylpropylamine)]perchlorate