2-(4-morpholinophenyl)ethanol

Base Information

• Chemical Name: 2-(4-morpholinophenyl)ethanol
• CAS No.: 105004-54-4
• Molecular Formula: C12H17NO2
• Molecular Weight: 207.272
• Hs Code.: 2934999090
• Mol file: 105004-54-4.mol

Synonyms:Morpholinomethyl-4-diphenylamin;4-Morpholin-4-ylmethyl-1H-quinolin-2-one;4-Morpholinophenethyl alcohol;4-Morpholinomethyl-carbostyril;4-Morpholinomethyl-diphenylamin;

Chemical Property of 2-(4-morpholinophenyl)ethanol

Chemical Property:

• Vapor Pressure: 1.55E-06mmHg at 25°C
• Boiling Point: 382.6oC at 760 mmHg
• Flash Point: 185.2oC
• PSA: 32.70000
• Density: 1.132g/cm3
• LogP: 1.12300

Purity/Quality:

98%min ^*data from raw suppliers

2-(4-MORPHOLINOPHENYL)ETHANOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-morpholinophenyl)ethanol

There total 2 articles about 2-(4-morpholinophenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

morpholine (110-91-8,99108-56-2) + 4-(2-(tetrahydropyran-2-yloxy)ethyl)bromobenzene (79849-46-0) → 4-(4-Morpholinyl)benzeneethanol (105004-54-4)

Guidance literature:

With johnphos; sodium t-butanolate; palladium diacetate; In toluene; at 70 ℃; for 16h;

Reference yield: 73.0%

morpholine (110-91-8,99108-56-2) + 4-bromophenethanol (4654-39-1) → 4-(4-Morpholinyl)benzeneethanol (105004-54-4)

Guidance literature:

With lithium hexamethyldisilazane; 2,8,9-tris(2-methylpropyl)-2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane; palladium diacetate; In tetrahydrofuran; toluene; at 80 ℃; for 26h;

DOI:10.1002/adsc.200404005

Reference yield:

(2S)-2-methyl-7-(morpholin-4-yl)-2-(trifluoromethyl)-2,3-dihydroimidazo[1,2-a]pyrimidin-5(1H)-one (1260983-00-3) + 4-(4-Morpholinyl)benzeneethanol (105004-54-4) → (S)-2-Methyl-7-morpholin-4-yl-1-[2-(4-morpholin-4-ylphenyl)ethyl]-2-trifluoromethyl-2,3-dihydro-1H-imidazo[1,2-a]pyrimidin-5-one (1260983-29-6)

Guidance literature:

With diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃;

upstream raw materials:

morpholine

4-bromophenethanol

4-(2-(tetrahydropyran-2-yloxy)ethyl)bromobenzene

Downstream raw materials:

(S)-2-Methyl-7-morpholin-4-yl-1-[2-(4-morpholin-4-ylphenyl)ethyl]-2-trifluoromethyl-2,3-dihydro-1H-imidazo[1,2-a]pyrimidin-5-one

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