(3S,6'S)-2,2,2-trichloroethyl spiro

Base Information

• Chemical Name: (3S,6'S)-2,2,2-trichloroethyl spiro
• CAS No.: 109706-76-5
• Molecular Formula: C₂₄H₂₂Cl₃N₃O₆S
• Molecular Weight: 586.88

Synonyms:

Chemical Property of (3S,6'S)-2,2,2-trichloroethyl spiro

Chemical Property:

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Technology Process of (3S,6'S)-2,2,2-trichloroethyl spiro

There total 1 articles about (3S,6'S)-2,2,2-trichloroethyl spiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

4-methoxy-N-(4-nitrobenzylidene)aniline (5455-87-8) + (2S,5R)-6-Diazo-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 2,2,2-trichloro-ethyl ester (51056-24-7) → (3S,6'S)-2,2,2-trichloroethyl spiro (109706-76-5)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 5 ℃; for 0.416667h;

Reference yield: 54.0%

(3S,6'S)-2,2,2-trichloroethyl spiro (109706-76-5) → (3S,7aR)-2,2,2-trichloroethyl 2,3,5,7a-tetrahydro-7-(4-methoxyphenylamino)-2,2-dimethyl-6-(4-nitrophenyl)-5-oxopyrrolo<2,1-b>thiazole-3-carboxylate (109706-81-2)

Guidance literature:

With boron trifluoride diethyl etherate; In chloroform; for 1.5h; Ambient temperature;

upstream raw materials:

4-methoxy-N-(4-nitrobenzylidene)aniline

(2S,5R)-6-Diazo-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 2,2,2-trichloro-ethyl ester

Downstream raw materials:

(3S,7aR)-2,2,2-trichloroethyl 2,3,5,7a-tetrahydro-7-(4-methoxyphenylamino)-2,2-dimethyl-6-(4-nitrophenyl)-5-oxopyrrolo<2,1-b>thiazole-3-carboxylate

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