C₂₂H₁₈O

Base Information

• Chemical Name: C₂₂H₁₈O
• CAS No.: 127903-33-7
• Molecular Formula: C₂₂H₁₈O
• Molecular Weight: 298.384
• Mol file: 127903-33-7.mol

Synonyms:

Chemical Property of C₂₂H₁₈O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₈O

There total 3 articles about C₂₂H₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

phenylmagnesium bromide (1589-82-8) + dibenzosuberenon (2222-33-5) → C22H18O (127903-33-7)

Guidance literature:

In tetrahydrofuran;

DOI:10.1002/jccs.201200570

Reference yield:

benzyl bromide (100-39-0) + dibenzosuberenon (2222-33-5) → C22H18O (127903-33-7)

Guidance literature:

benzyl bromide; With magnesium; In diethyl ether; for 2.16667h; Reflux;

dibenzosuberenon; In diethyl ether; for 2.16667h; Reflux;

With water; ammonium chloride; In diethyl ether;

DOI:10.1021/jo200227t

Reference yield:

5-Allyl-dibenzo-cyclohepten-5-ol (16203-85-3) → C22H18O (127903-33-7)

Guidance literature:

Multi-step reaction with 2 steps

1: ethyl acetate / 2 h / 20 °C / Inert atmosphere; Photolysis

2: tetrahydrofuran

In tetrahydrofuran; ethyl acetate;

DOI:10.1002/jccs.201200570

upstream raw materials:

benzyl bromide

dibenzosuberenon

phenylmagnesium bromide

5-Allyl-dibenzo-cyclohepten-5-ol

Downstream raw materials:

5-benzylidene-5H-dibenzo[a,d]cycloheptene