C₄₁H₅₇N₇O₉S

Base Information

• Chemical Name: C₄₁H₅₇N₇O₉S
• CAS No.: 1273327-76-6
• Molecular Formula: C₄₁H₅₇N₇O₉S
• Molecular Weight: 824.011
• Mol file: 1273327-76-6.mol

Synonyms:

Chemical Property of C₄₁H₅₇N₇O₉S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₅₇N₇O₉S

There total 6 articles about C₄₁H₅₇N₇O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C40H52N6O7S (1355586-15-0) → C41H57N7O9S (1273327-76-6)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

2: palladium on activated charcoal; hydrogen / methanol

3: 1-hydroxy-7-aza-benzotriazole; potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; potassium hydrogencarbonate; HATU; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/cbic.201000572

Reference yield:

C56H71N7O12S (1273327-67-5) → C41H57N7O9S (1273327-76-6)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol

2: 1-hydroxy-7-aza-benzotriazole; potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; potassium hydrogencarbonate; HATU; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/cbic.201000572

Reference yield:

Nα-Fmoc-N(G)-(2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl)-L-arginine benzyl ester (1076089-07-0) → C41H57N7O9S (1273327-76-6)

Guidance literature:

Multi-step reaction with 5 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2: potassium carbonate; thiophenol / acetonitrile / 2 h / 20 °C

3: potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

4: palladium on activated charcoal; hydrogen / methanol

5: 1-hydroxy-7-aza-benzotriazole; potassium hydrogencarbonate; HATU / N,N-dimethyl-formamide

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; potassium carbonate; benzotriazol-1-ol; potassium hydrogencarbonate; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; HATU; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/cbic.201000572

upstream raw materials:

Nα-Fmoc-N(G)-(2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl)-L-arginine benzyl ester

C₄₆H₅₅N₇O₁₁S₂

C₄₀H₅₂N₆O₇S

C₅₆H₇₁N₇O₁₂S

Downstream raw materials:

C₂₄H₃₃N₇O₆