N-ALPHA-TRITYL-L-VALINE DIETHYLAMINE

Base Information

• Chemical Name: N-ALPHA-TRITYL-L-VALINE DIETHYLAMINE
• CAS No.: 3485-55-0
• Molecular Formula: C₄H₁₁N*C₂₄H₂₅NO₂
• Molecular Weight: 432.606
• Mol file: 3485-55-0.mol

Synonyms:

Chemical Property of N-ALPHA-TRITYL-L-VALINE DIETHYLAMINE

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

N-ALPHA-TRITYL-L-VALINE DIETHYLAMMONIUM SALT 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-ALPHA-TRITYL-L-VALINE DIETHYLAMINE

There total 3 articles about N-ALPHA-TRITYL-L-VALINE DIETHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trityl chloride (76-83-5) + D,L-valine (516-06-3,25609-85-2,7004-03-7,921-10-8) + diethylamine (109-89-7) → Trit-Val-OH.Et2NH (3485-55-0)

Guidance literature:

With bis-(trimethylsilyl)acetamide; triethylamine; Yield given. Multistep reaction; 1.) DMFA, 2.) O deg C, 2h, room temp., 6h, 3.) Et₂O;

DOI:10.1007/BF00580560

Reference yield:

N,O-bis(trimethylsilyl)-L-valine (7364-44-5) + trityl chloride (76-83-5) + diethylamine (109-89-7) → Trt-Val*Et2NH (3485-55-0)

Guidance literature:

Yield given. Multistep reaction; 1.) CHCl₃, 1 h, reflux;

Reference yield:

→ Trit-Val-OH.Et2NH (3485-55-0)

Guidance literature:

Tritylchlorid, L-Valin, Diethylamin;

DOI:10.1515/znb-1970-0326

upstream raw materials:

trityl chloride

D,L-valine

diethylamine

N,O-bis(trimethylsilyl)-L-valine

Refernces

• 1、 Mamos, Petros,Sanida, Chariklia,Barlos, Kleomenis. "Preparation of N-Tritylamino Acids from N-Trimethylsilylamino Acid Trimethylsilyl Esters". . p. 1083 - 1084. Retrieved 2007/10/02.