C₂₅H₃₃FN₂O₆S

Base Information

Chemical Name:C₂₅H₃₃FN₂O₆S
CAS No.:1367877-83-5
Molecular Formula:C₂₅H₃₃FN₂O₆S
Molecular Weight:508.611
Hs Code.:

C<sub>25</sub>H<sub>33</sub>FN<sub>2</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₂₅H₃₃FN₂O₆S

Chemical Property:

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Technology Process of C₂₅H₃₃FN₂O₆S

There total 13 articles about C₂₅H₃₃FN₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1123173-00-1
(3R,4S,5S)-3-((3-(tert-butyl)benzyl)-amino)-5-(3,5-difluoro-4-nitrobenzyl)-4-hydroxytetrahydro-2H-thiothiopyran

: 1367877-83-5
C₂₅H₃₃FN₂O₆S

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / 1,4-dioxane / 2 h / 25 °C / Inert atmosphere

2.1: sodium acetate / methanol; dichloromethane / 0.5 h / 25 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

2.3: 0.25 h / Inert atmosphere

3.1: potassium hydroxide / tetrahydrofuran / 0.33 h / Microwave irradiation

With hydrogenchloride; sodium acetate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jm300069y

Reference yield:

: 67567-26-4
4-bromo-2,6-difluoroaniline

: 1367877-83-5
C₂₅H₃₃FN₂O₆S

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium perborate; acetic acid / 21 h / 65 - 70 °C / Inert atmosphere

2.1: 1-methyl-pyrrolidin-2-one / 6 h / 160 - 165 °C / Inert atmosphere

3.1: thionyl chloride / 0 - 25 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4 h / 0 - 5 °C / Inert atmosphere

4.2: 0.5 h / 25 °C / Cooling with ice; Inert atmosphere

5.1: phosphorus tribromide / 24 h / 25 °C / Inert atmosphere

6.1: potassium carbonate / acetone / 2.5 h / 25 - 30 °C / Inert atmosphere

7.1: palladium diacetate; triethylamine; triphenylphosphine / tert-butyl methyl ether / 16 h / 25 °C / Inert atmosphere

8.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -70 °C / Inert atmosphere

9.1: Chiralpak AD-I / ethanol; n-heptane / Inert atmosphere

10.1: potassium peroxymonosulfate / tetrahydrofuran; water / 2 h / 40 °C / Inert atmosphere

11.1: hydrogenchloride / 1,4-dioxane / 2 h / 25 °C / Inert atmosphere

12.1: sodium acetate / methanol; dichloromethane / 0.5 h / 25 °C / Inert atmosphere

12.2: 1 h / Inert atmosphere

12.3: 0.25 h / Inert atmosphere

13.1: potassium hydroxide / tetrahydrofuran / 0.33 h / Microwave irradiation

With 1-methyl-pyrrolidin-2-one; hydrogenchloride; sodium perborate; lithium aluminium tetrahydride; thionyl chloride; potassium peroxymonosulfate; sodium acetate; palladium diacetate; phosphorus tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; n-heptane; dichloromethane; tert-butyl methyl ether; water; acetone;
DOI:10.1021/jm300069y

Reference yield:

: 1123172-88-2
3,5-difluoro-4-nitro-benzonitrile

: 1367877-83-5
C₂₅H₃₃FN₂O₆S

Guidance literature:: Multi-step reaction with 11 steps

1.1: thionyl chloride / 0 - 25 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4 h / 0 - 5 °C / Inert atmosphere

2.2: 0.5 h / 25 °C / Cooling with ice; Inert atmosphere

3.1: phosphorus tribromide / 24 h / 25 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 2.5 h / 25 - 30 °C / Inert atmosphere

5.1: palladium diacetate; triethylamine; triphenylphosphine / tert-butyl methyl ether / 16 h / 25 °C / Inert atmosphere

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -70 °C / Inert atmosphere

7.1: Chiralpak AD-I / ethanol; n-heptane / Inert atmosphere

8.1: potassium peroxymonosulfate / tetrahydrofuran; water / 2 h / 40 °C / Inert atmosphere

9.1: hydrogenchloride / 1,4-dioxane / 2 h / 25 °C / Inert atmosphere

10.1: sodium acetate / methanol; dichloromethane / 0.5 h / 25 °C / Inert atmosphere

10.2: 1 h / Inert atmosphere

10.3: 0.25 h / Inert atmosphere

11.1: potassium hydroxide / tetrahydrofuran / 0.33 h / Microwave irradiation

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; potassium peroxymonosulfate; sodium acetate; palladium diacetate; phosphorus tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; n-heptane; dichloromethane; tert-butyl methyl ether; water; acetone;
DOI:10.1021/jm300069y