tetrabenzyltitanium-d28

Base Information

Chemical Name:tetrabenzyltitanium-d28
CAS No.:59512-61-7
Molecular Formula:C₂₈H₂₈Ti
Molecular Weight:440.188
Hs Code.:

Synonyms:

Suppliers and Price of tetrabenzyltitanium-d28

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetrabenzyltitanium-d28

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetrabenzyltitanium-d28

There total 1 articles about tetrabenzyltitanium-d28 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 59502-05-5
benzyl chloride-d7

: 7550-45-0
titanium tetrachloride

: 59512-61-7
tetrabenzyltitanium-d28

Guidance literature:: With Mg; In diethyl ether; (inert atm., glovebox technique); addn. of magnesium to ethereal soln. of benzyl chloride, filtration, addn. of titanium compd., stirring at room temp. overnight; filtration through celite, evapn., addn. of petroleum ether, filtration,crystn. at -35°C overnight, NMR;
DOI:10.1021/om100253u

Reference yield: 25.0%

: 1015257-52-9
C₆H₄(C₆H₂(CH₃)(CMe₃)OH)2

: 59512-61-7
tetrabenzyltitanium-d28

: [(C₆H₄(C₆H₂(CH₃)(CMe₃)O)2)Ti(benzyl-d7)2]

Guidance literature:: In toluene; (inert atm., glovebox technique); addn. of toluene soln. of phenol deriv. to toluene soln. of titanium compd., stirring for 1 h; evapn., addn. of petroleum ether or pentane, filtration, crystn. at -35°C for few ds, NMR;
DOI:10.1021/om100253u