bis(1,2-di(4-methylphenyl)ethylene-1,2-dithiolate)nickel

Base Information

Chemical Name:bis(1,2-di(4-methylphenyl)ethylene-1,2-dithiolate)nickel
CAS No.:89918-29-6
Molecular Formula:C₃₂H₂₈NiS₄
Molecular Weight:599.528
Hs Code.:

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Chemical Property of bis(1,2-di(4-methylphenyl)ethylene-1,2-dithiolate)nickel

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Technology Process of bis(1,2-di(4-methylphenyl)ethylene-1,2-dithiolate)nickel

There total 1 articles about bis(1,2-di(4-methylphenyl)ethylene-1,2-dithiolate)nickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.1%

: nickel(II) chloride hexahydrate

: 3457-48-5
1,2-di(4-methylphenyl)-1,2-ethanedione

: phosphorous (V) sulfide

: 89918-29-6
bis(1,2-di(4-methylphenyl)ethylene-1,2-dithiolate)nickel

Guidance literature:: In 1,4-dioxane; water; ligand refluxed with P2S5 for 6 h, filtered while hot, aq. soln. of NiCl2 added (5:7.5:2.5 molar ratio), refluxed for 2-4 h; crystd. on cooling, crystd., filtered off, washed (dioxane, H2O, EtOH, ether), dried, recrystd. (DCM), elem. anal.;
DOI:10.1016/j.ica.2011.07.046