2,4-diphenyl-1,3,2,4-diselenastilbetane

Base Information

• Chemical Name: 2,4-diphenyl-1,3,2,4-diselenastilbetane
• CAS No.: 895166-04-8
• Molecular Formula: C₁₂H₁₀Sb₂Se₂
• Molecular Weight: 555.631
• Mol file: 895166-04-8.mol

Synonyms:

Chemical Property of 2,4-diphenyl-1,3,2,4-diselenastilbetane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-diphenyl-1,3,2,4-diselenastilbetane

There total 3 articles about 2,4-diphenyl-1,3,2,4-diselenastilbetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

piperidine (110-89-4) + bis[(4-methylbenzoyl)seleno]phenylantimony → 2,4-diphenyl-1,3,2,4-diselenastilbetane (895166-04-8) + di(piperidinium) phenylstibonoselenoite

Guidance literature:

In diethyl ether; byproducts: N-(4-methylbenzoyl)piperidine; to a suspn. of Sb-compound in diethyl ether was added a soln. of piperidine in diethyl ether at room temp., the mixt. was stirred at 0°C for 1 h; evapd., chromy. on silica gel (diethyl ether);

DOI:10.1002/hlca.200690070

Reference yield:

dichlorophenylstibine (5035-52-9) → 2,4-diphenyl-1,3,2,4-diselenastilbetane (895166-04-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: diethyl ether

In diethyl ether; dichloromethane;

DOI:10.1002/hlca.200690070

Reference yield:

dichlorophenylstibine (5035-52-9) + sodium 4-methylbenzenecarboselenoate (128816-64-8) → 2,4-diphenyl-1,3,2,4-diselenastilbetane (895166-04-8) + di(piperidinium) phenylstibonoselenoite

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: diethyl ether

In diethyl ether; dichloromethane;

DOI:10.1002/hlca.200690070

upstream raw materials:

piperidine

dichlorophenylstibine

sodium 4-methylbenzenecarboselenoate

Refernces