C₂₆H₂₅F₃N₄O₂

Base Information

Chemical Name:C₂₆H₂₅F₃N₄O₂
CAS No.:1417538-98-7
Molecular Formula:C₂₆H₂₅F₃N₄O₂
Molecular Weight:482.505
Hs Code.:

C<sub>26</sub>H<sub>25</sub>F<sub>3</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₆H₂₅F₃N₄O₂

Chemical Property:

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Technology Process of C₂₆H₂₅F₃N₄O₂

There total 5 articles about C₂₆H₂₅F₃N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870843-27-9
C₁₇H₁₉ClN₂O₃

: 1417538-98-7
C₂₆H₂₅F₃N₄O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

2: sodium methylate / methanol

3: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 80 °C

4: hydrazine / acetonitrile

5: phosphorus pentoxide / ethanol / 80 °C

With tributylphosphine; phosphorus pentoxide; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; acetonitrile; 3: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.11.055

Reference yield:

: 870843-25-7
5-chloro-2-(diethoxyphosphoryl)valeric acid tert-butyl ester

: 1417538-98-7
C₂₆H₂₅F₃N₄O₂

Guidance literature:: Multi-step reaction with 7 steps

1: lithium hydroxide / tetrahydrofuran

2: trifluoroacetic acid

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

4: sodium methylate / methanol

5: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 80 °C

6: hydrazine / acetonitrile

7: phosphorus pentoxide / ethanol / 80 °C

With tributylphosphine; phosphorus pentoxide; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; lithium hydroxide; hydrazine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; acetonitrile; 1: |Wittig Olefination / 5: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.11.055

Reference yield:

: C₂₆H₂₇ClF₃N₃O₃

: 1417538-98-7
C₂₆H₂₅F₃N₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1: sodium methylate / methanol

2: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 80 °C

3: hydrazine / acetonitrile

4: phosphorus pentoxide / ethanol / 80 °C

With tributylphosphine; phosphorus pentoxide; sodium methylate; hydrazine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; ethanol; acetonitrile; 2: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.11.055