Technology Process of C48H73F2N5O17
There total 5 articles about C48H73F2N5O17 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: silver(l) oxide / acetonitrile / 4 h / 0 °C / Darkness
2: diethylamino-sulfur trifluoride / dichloromethane / 8 h / 20 °C / Inert atmosphere
3: hydrogen; palladium 10% on activated carbon / acetonitrile / 20 °C / 1368.09 Torr
4: potassium carbonate / dichloromethane / Cooling with ice
5: triethylamine / acetonitrile / 24 h / 70 °C
With
diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; silver(l) oxide;
In
dichloromethane; acetonitrile;
DOI:10.1021/ic301827p
- Guidance literature:
-
Multi-step reaction with 5 steps
1: silver(l) oxide / acetonitrile / 4 h / 0 °C / Darkness
2: diethylamino-sulfur trifluoride / dichloromethane / 8 h / 20 °C / Inert atmosphere
3: hydrogen; palladium 10% on activated carbon / acetonitrile / 20 °C / 1368.09 Torr
4: potassium carbonate / dichloromethane / Cooling with ice
5: triethylamine / acetonitrile / 24 h / 70 °C
With
diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; silver(l) oxide;
In
dichloromethane; acetonitrile;
DOI:10.1021/ic301827p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethylamino-sulfur trifluoride / dichloromethane / 8 h / 20 °C / Inert atmosphere
2: hydrogen; palladium 10% on activated carbon / acetonitrile / 20 °C / 1368.09 Torr
3: potassium carbonate / dichloromethane / Cooling with ice
4: triethylamine / acetonitrile / 24 h / 70 °C
With
diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine;
In
dichloromethane; acetonitrile;
DOI:10.1021/ic301827p