4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

Base Information

Chemical Name:4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine
CAS No.:135300-31-1
Molecular Formula:C₂₃H₁₉ClN₆S
Molecular Weight:446.963
Hs Code.:
Mol file:135300-31-1.mol

Synonyms:

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Chemical Property of 4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

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Technology Process of 4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

There total 5 articles about 4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 135300-24-2
4-hydrazino-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

: 123-54-6,81235-32-7
acetylacetone

: 135300-31-1
4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

Guidance literature:: In ethanol; for 3h; Heating;

Reference yield:

: 94833-68-8
3-amino-4-(p-chlorophenyl)-5,6,7,8-tetrahydrothieno<2,3-b>quinoline-2-carbonitrile

: 135300-31-1
4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / CH₃COOH, conc. HCl, NaNO₂ / H₂O / 2 h

2: 91 percent / thiourea / methanol / 3 h / Heating

3: 83 percent / 5percent NaOH / 2 h

4: 94 percent / hydrazine hydrate / ethanol / 3 h / Heating

5: 90 percent / ethanol / 3 h / Heating

With hydrogenchloride; sodium hydroxide; hydrazine hydrate; acetic acid; thiourea; sodium nitrite; In methanol; ethanol; water;

Reference yield:

: 135300-22-0
4-chloro-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

: 135300-31-1
4-(3,5-dimethylpyrazol-1-yl)-11-p-chlorophenyl-7,8,9,10-tetrahydro-equinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / thiourea / methanol / 3 h / Heating

2: 83 percent / 5percent NaOH / 2 h

3: 94 percent / hydrazine hydrate / ethanol / 3 h / Heating

4: 90 percent / ethanol / 3 h / Heating

With sodium hydroxide; hydrazine hydrate; thiourea; In methanol; ethanol;