C₂₄H₃₈N₂O₅Si

Base Information

Chemical Name:C₂₄H₃₈N₂O₅Si
CAS No.:1392005-88-7
Molecular Formula:C₂₄H₃₈N₂O₅Si
Molecular Weight:462.662
Hs Code.:

C<sub>24</sub>H<sub>38</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₂₄H₃₈N₂O₅Si

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Technology Process of C₂₄H₃₈N₂O₅Si

There total 7 articles about C₂₄H₃₈N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1392005-87-6
C₁₉H₃₀N₂O₅Si

: 630-19-3
pivalaldehyde

: 1392005-88-7
C₂₄H₃₈N₂O₅Si

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/om300442e

Reference yield:

: 18141-66-7
diethyl methyl[(trimethylsilyl)methyl]malonate

: 1392005-88-7
C₂₄H₃₈N₂O₅Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: porcine liver esterase; water / 94 h / 38 °C / Enzymatic reaction

2.1: sulfuric acid / dichloromethane / -20 - 20 °C / Inert atmosphere; Enzymatic reaction

2.2: 54 h / Inert atmosphere; Reflux

3.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

4.1: sodium azide / acetone / 0 - 20 °C / Inert atmosphere

5.1: acetone / 16 h / Inert atmosphere; Reflux

6.1: hydrogenchloride / water / 16 h / Reflux

7.1: sodium hydroxide / water; methanol / 24 h / 10 °C / Inert atmosphere

8.1: thionyl chloride / -20 °C / Inert atmosphere; Reflux

9.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 4-methyl-morpholine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

10.1: chloro-trimethyl-silane; phenol / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

10.2: Inert atmosphere

11.1: magnesium sulfate / dichloromethane / 24 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; porcine liver esterase; chloro-trimethyl-silane; thionyl chloride; sodium azide; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); sulfuric acid; water; magnesium sulfate; sodium hydroxide; phenol; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/om300442e

Reference yield:

: C₁₁H₂₅NO₂Si

: 1392005-88-7
C₂₄H₃₈N₂O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / water / 16 h / Reflux

2.1: sodium hydroxide / water; methanol / 24 h / 10 °C / Inert atmosphere

3.1: thionyl chloride / -20 °C / Inert atmosphere; Reflux

4.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 4-methyl-morpholine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: chloro-trimethyl-silane; phenol / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

5.2: Inert atmosphere

6.1: magnesium sulfate / dichloromethane / 24 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; chloro-trimethyl-silane; thionyl chloride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); magnesium sulfate; sodium hydroxide; phenol; In methanol; dichloromethane; water;
DOI:10.1021/om300442e