mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose

Base Information

Chemical Name:mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose
CAS No.:1574535-47-9
Molecular Formula:C₆₉H₇₀O₁₆S₂Si
Molecular Weight:1247.52
Hs Code.:

mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose

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Technology Process of mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose

There total 4 articles about mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1574535-39-9
mecapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranoside

: 98-88-4
benzoyl chloride

: 1574535-47-9
mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose

Guidance literature:: With pyridine; 1-methyl-1H-imidazole; for 48h;
DOI:10.1039/c3ob42194e

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1574535-47-9
mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 48 h

2: boron trifluoride diethyl etherate / dichloromethane / 1.5 h / 0 °C / Molecular sieve

3: pyridine; 1-methyl-1H-imidazole / 48 h

With pyridine; 1-methyl-1H-imidazole; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1039/c3ob42194e

Reference yield:

: mecapto-tert-butyl 1-thio-D-mannopyranoside

: 1574535-47-9
mercapto-tert-butyl 2-O-acetyl-3,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1→3)-2,4-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 48 h

2: boron trifluoride diethyl etherate / dichloromethane / 1.5 h / 0 °C / Molecular sieve

3: pyridine; 1-methyl-1H-imidazole / 48 h

With pyridine; 1-methyl-1H-imidazole; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1039/c3ob42194e