toxogonin

Base Information

• Chemical Name: toxogonin
• CAS No.: 24275-90-9
• Molecular Formula: C₁₄H₁₆N₄O₃*2Cl
• Molecular Weight: 359.212
• Mol file: 24275-90-9.mol

Synonyms:

Chemical Property of toxogonin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of toxogonin

There total 3 articles about toxogonin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

pyridine-4-carbaldehyde (872-85-5) + bis(2-chloromethyl)ether (542-88-1) → toxogonin (114-90-9,5046-13-9,24275-90-9,24275-91-0)

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 6h; Sealed tube;

DOI:10.1016/j.cbi.2019.05.048

Reference yield:

→ obidoxime chloride (114-90-9,5046-13-9,24275-90-9,24275-91-0)

Guidance literature:

Pyridin-4-aldoxim, Bis-chlormethylether, wfr. CHCl3, 50grad;

Reference yield:

→ obidoxime (114-90-9,5046-13-9,24275-90-9,24275-91-0)

Guidance literature:

Pyridin-4-aldoxim, Bis-chlormethylether, wfr. CHCl3, 50grad;

upstream raw materials:

pyridine-4-carbaldehyde

bis(2-chloromethyl)ether

Downstream raw materials:

O-(O,O-diethylphosphoryl)obidoxime

4-nitro-phenol