(3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

Base Information

Chemical Name:(3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene
CAS No.:186900-91-4
Molecular Formula:C₃₃H₄₁NO₄SeSi
Molecular Weight:622.738
Hs Code.:

(3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

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Technology Process of (3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

There total 5 articles about (3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 136787-49-0
3-(tert-butyldiphenylsilyloxy)prop-1-ene

: 186900-89-0
(3aR,4R,6aS)-2,2-Dimethyl-4-phenylselanylmethyl-4,6a-dihydro-3aH-[1,3]dioxolo[4,5-c]pyrrole 5-oxide

: (3aS,3bS,4R,7R,7aR)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

: (3aS,3bS,5R,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

: 186900-91-4
(3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1055/s-1997-695

Reference yield:

: 114817-96-8,127758-25-2,99902-67-7
(4S,5R)-2,2-dimethyl-4-hydroxymethyl-5-vinyl-1,3-dioxolane

: 186900-91-4
(3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 4 steps

1: (COCl)2, DMSO / CH₂Cl₂ / -60 °C

2: NH₂OH

3: CH₂Cl₂

4: 72 percent / toluene / 2 h / Heating

With oxalyl dichloride; hydroxylamine; dimethyl sulfoxide; In dichloromethane; toluene;
DOI:10.1055/s-1997-695

Reference yield:

: 155934-55-7
(4R,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolane-4-carbaldehyde

: 186900-91-4
(3aS,3bS,5S,7R,7aR)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-7-phenylselanylmethyl-hexahydro-1,3,6-trioxa-6a-aza-cyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂OH

2: CH₂Cl₂

3: 72 percent / toluene / 2 h / Heating

With hydroxylamine; In dichloromethane; toluene;
DOI:10.1055/s-1997-695