1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan

Base Information

Chemical Name:1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan
CAS No.:73920-88-4
Molecular Formula:C₃₁H₅₇N₃O₂S
Molecular Weight:535.878
Hs Code.:

Synonyms:

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Chemical Property of 1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan

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Technology Process of 1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan

There total 7 articles about 1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 373-44-4
1,8-diaminooctan

: 73920-88-4
1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / toluene / 0 - 2 °C

2: 1.) 1N BH₃, 2.) 6N HCl / 1.) THF, 1 h, room temp., 2 h, reflux, 2.) ethanol, 1 h, reflux

With hydrogenchloride; borane; In toluene;

Reference yield:

: 26825-92-3
methyl 8-bromooctanoate

: 73920-88-4
1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Na, 2.) potassium t-butylate / 1.) DMSO, 14 h, room temp., 2.) 48 h, DMSO

2: 50percent NaOH / ethanol / 2 h / Heating

3: 93 percent / oxalyl chloride / benzene / 48 h / Ambient temperature

4: 40 percent / toluene / 0 - 2 °C

5: 1.) 1N BH₃, 2.) 6N HCl / 1.) THF, 1 h, room temp., 2 h, reflux, 2.) ethanol, 1 h, reflux

With hydrogenchloride; sodium hydroxide; oxalyl dichloride; borane; potassium tert-butylate; sodium; In ethanol; toluene; benzene;

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 73920-88-4
1<(4-Methylphenyl)sulfonyl>-1,10,19-triazacyclohepteicosan

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Na, 2.) potassium t-butylate / 1.) DMSO, 14 h, room temp., 2.) 48 h, DMSO

2: 50percent NaOH / ethanol / 2 h / Heating

3: 93 percent / oxalyl chloride / benzene / 48 h / Ambient temperature

4: 40 percent / toluene / 0 - 2 °C

5: 1.) 1N BH₃, 2.) 6N HCl / 1.) THF, 1 h, room temp., 2 h, reflux, 2.) ethanol, 1 h, reflux

With hydrogenchloride; sodium hydroxide; oxalyl dichloride; borane; potassium tert-butylate; sodium; In ethanol; toluene; benzene;