4-Oxazolecarboxylic acid, 2-[[6-(2-methyl-3-oxo-1-propenyl)-2-(2,4,6-trimethylphenyl)-1,3-dioxan-4 -yl]methyl]-, methyl ester

Base Information

Chemical Name:4-Oxazolecarboxylic acid, 2-[[6-(2-methyl-3-oxo-1-propenyl)-2-(2,4,6-trimethylphenyl)-1,3-dioxan-4 -yl]methyl]-, methyl ester
CAS No.:105228-55-5
Molecular Formula:C23H27NO6
Molecular Weight:413.47
Hs Code.:
Mol file:105228-55-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Oxazolecarboxylic acid, 2-[[6-(2-methyl-3-oxo-1-propenyl)-2-(2,4,6-trimethylphenyl)-1,3-dioxan-4 -yl]methyl]-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Oxazolecarboxylic acid, 2-[[6-(2-methyl-3-oxo-1-propenyl)-2-(2,4,6-trimethylphenyl)-1,3-dioxan-4 -yl]methyl]-, methyl ester

There total 8 articles about 4-Oxazolecarboxylic acid, 2-[[6-(2-methyl-3-oxo-1-propenyl)-2-(2,4,6-trimethylphenyl)-1,3-dioxan-4 -yl]methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 24720-64-7
2-(triphenylphosphoranylidene)propionaldehyde

: 105228-54-4
2-[(4R,6S)-6-Formyl-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-ylmethyl]-oxazole-4-carboxylic acid methyl ester

: 105228-55-5
2-[(4R,6S)-6-((E)-2-Methyl-3-oxo-propenyl)-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-ylmethyl]-oxazole-4-carboxylic acid methyl ester

Guidance literature:: In benzene; for 23h; Heating;
DOI:10.1021/ja954312r

Reference yield:

: 105228-53-3
2-[(4R,6S)-6-Hydroxymethyl-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-ylmethyl]-oxazole-4-carboxylic acid methyl ester

: 105228-55-5
2-[(4R,6S)-6-((E)-2-Methyl-3-oxo-propenyl)-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-ylmethyl]-oxazole-4-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / SO₃*pyridine, Et₃N / dimethylsulfoxide

2: 82 percent / benzene / 23 h / Heating

With pyridine-SO₃ complex; triethylamine; In dimethyl sulfoxide; benzene;
DOI:10.1021/ja954312r

Reference yield:

: 64761-29-1
mesitaldehyde dimethylacetal

: 105228-55-5
2-[(4R,6S)-6-((E)-2-Methyl-3-oxo-propenyl)-2-(2,4,6-trimethyl-phenyl)-[1,3]dioxan-4-ylmethyl]-oxazole-4-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / camphorsulfonic acid / CH₂Cl₂ / 48 h / 0 °C

2: 86 percent / SO₃*pyridine, Et₃N / dimethylsulfoxide

3: 82 percent / benzene / 23 h / Heating

With pyridine-SO₃ complex; camphor-10-sulfonic acid; triethylamine; In dichloromethane; dimethyl sulfoxide; benzene;
DOI:10.1021/ja954312r