4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone

Base Information

Chemical Name:4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone
CAS No.:129355-82-4
Molecular Formula:C₂₇H₃₃ClN₂O₅
Molecular Weight:501.022
Hs Code.:

4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-<N-(3-methoxycarbopropionyl)methylamino>butyrophenone

Synonyms:

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Chemical Property of 4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone

Chemical Property:

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Technology Process of 4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone

There total 5 articles about 4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39512-49-7
4-(4-chlorophenyl)-4-hydroxypiperidine

: 129355-82-4
4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 16.42 g / KI / various solvent(s) / 7 h / Heating

2: 13.34 g / 10percent aq. NaOH / ethanol / 15 h / Heating

3: 8.34 g / pyridine / diethyl ether / 2.5 h

With pyridine; sodium hydroxide; potassium iodide; In diethyl ether; ethanol;
DOI:10.1002/jps.2600790515

Reference yield:

: 129355-78-8
4'-(cyclopropylcarbonyl)-N-methylacetanilide

: 129355-82-4
4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 15.8 g / HCl / propan-2-ol; H₂O / 7 h / Ambient temperature

2: 16.42 g / KI / various solvent(s) / 7 h / Heating

3: 13.34 g / 10percent aq. NaOH / ethanol / 15 h / Heating

4: 8.34 g / pyridine / diethyl ether / 2.5 h

With pyridine; hydrogenchloride; sodium hydroxide; potassium iodide; In diethyl ether; ethanol; water; isopropyl alcohol;
DOI:10.1002/jps.2600790515

Reference yield:

: 129355-79-9
4-chloro-4'-(N-methylacetamido)butyrophenone

: 129355-82-4
4-<4-(p-chlorophenyl)-4-hydroxypiperidino>-4'-butyrophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 16.42 g / KI / various solvent(s) / 7 h / Heating

2: 13.34 g / 10percent aq. NaOH / ethanol / 15 h / Heating

3: 8.34 g / pyridine / diethyl ether / 2.5 h

With pyridine; sodium hydroxide; potassium iodide; In diethyl ether; ethanol;
DOI:10.1002/jps.2600790515