N-[(Diethylcarbamothioyl)sulfanyl]-4-methoxybenzamide

Base Information

Chemical Name:N-[(Diethylcarbamothioyl)sulfanyl]-4-methoxybenzamide
CAS No.:105246-30-8
Molecular Formula:C13H18N2O2S2
Molecular Weight:298.43
Hs Code.:
DSSTox Substance ID:DTXSID70546001
Nikkaji Number:J433.836G
Wikidata:Q82423684
Mol file:105246-30-8.mol

Synonyms:105246-30-8;N-[(Diethylcarbamothioyl)sulfanyl]-4-methoxybenzamide;DTXSID70546001

Suppliers and Price of N-[(Diethylcarbamothioyl)sulfanyl]-4-methoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[(Diethylcarbamothioyl)sulfanyl]-4-methoxybenzamide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:298.08097017
Heavy Atom Count:19
Complexity:301

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=S)SNC(=O)C1=CC=C(C=C1)OC

Technology Process of N-[(Diethylcarbamothioyl)sulfanyl]-4-methoxybenzamide

There total 2 articles about N-[(Diethylcarbamothioyl)sulfanyl]-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106860-28-0
S-diethylthiocarbamoyl-substituted sulfenamide

: 100-07-2
4-methoxy-benzoyl chloride

: 105246-30-8
C₁₃H₁₈N₂O₂S₂

Guidance literature:: With sodium hydroxide; In diethyl ether; at 10 ℃; for 3h;
DOI:10.1246/bcsj.59.2017

Reference yield:

: 3424-93-9
4-methoxyphenylacetamide

: 105246-30-8
C₁₃H₁₈N₂O₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride, 2.) iodine / 1.) THF, RT, 1 h, 2.) THF, RT, 15 min

2: tetrahydrofuran / 1 h / Ambient temperature

With iodine; sodium hydride; In tetrahydrofuran;
DOI:10.1246/bcsj.64.3732