C₂₃H₂₆INO₃

Base Information

Chemical Name:C₂₃H₂₆INO₃
CAS No.:1434686-56-2
Molecular Formula:C₂₃H₂₆INO₃
Molecular Weight:491.369
Hs Code.:

C<sub>23</sub>H<sub>26</sub>INO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₆INO₃

Chemical Property:

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Technology Process of C₂₃H₂₆INO₃

There total 9 articles about C₂₃H₂₆INO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1349820-67-2
6-butyl-3-iodo-2-methyl-7-(2-phenoxyethoxy)quinolin-4(1H)-one

: 74-88-4
methyl iodide

: 1434686-56-2
C₂₃H₂₆INO₃

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 5h;

Reference yield:

: 621-42-1
meta-hydroxyacetanilide

: 1434686-56-2
C₂₃H₂₆INO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine / 18.5 h / 20 °C

2.1: aluminum (III) chloride / 3.75 h / 150 - 175 °C

3.1: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / 0 °C

4.1: palladium 10% on activated carbon; hydrogen / acetic acid / 11 h / 3102.97 Torr

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

5.2: 4 h / 75 °C / Inert atmosphere

6.1: potassium hydroxide / ethanol; water / 18 h / 0 °C / Reflux

7.1: acetic acid / benzene / Dean-Stark; Reflux

7.2: 0.25 h / Reflux

8.1: iodine; sodium hydroxide / methanol / 20 °C

9.1: caesium carbonate / N,N-dimethyl-formamide / 5 h / 0 - 20 °C

With aluminum (III) chloride; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; iodine; sodium hydride; caesium carbonate; acetic acid; potassium hydroxide; sodium hydroxide; In pyridine; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 28583-62-2
N-(4-butyryl-3-hydroxyphenyl)acetamide

: 1434686-56-2
C₂₃H₂₆INO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / 0 °C

2.1: palladium 10% on activated carbon; hydrogen / acetic acid / 11 h / 3102.97 Torr

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

3.2: 4 h / 75 °C / Inert atmosphere

4.1: potassium hydroxide / ethanol; water / 18 h / 0 °C / Reflux

5.1: acetic acid / benzene / Dean-Stark; Reflux

5.2: 0.25 h / Reflux

6.1: iodine; sodium hydroxide / methanol / 20 °C

7.1: caesium carbonate / N,N-dimethyl-formamide / 5 h / 0 - 20 °C

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; iodine; sodium hydride; caesium carbonate; acetic acid; potassium hydroxide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; benzene;