9--Δ^4a-dodecahydro-phenanthren-carbonsaeure-(10)

Base Information

• Chemical Name: 9--Δ^4a-dodecahydro-phenanthren-carbonsaeure-(10)
• CAS No.: 97013-75-7
• Molecular Formula: C₂₇H₃₀O₂
• Molecular Weight: 386.534

Synonyms:

Chemical Property of 9--Δ^4a-dodecahydro-phenanthren-carbonsaeure-(10)

Chemical Property:

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Technology Process of 9--Δ^4a-dodecahydro-phenanthren-carbonsaeure-(10)

There total 1 articles about 9--Δ^4a-dodecahydro-phenanthren-carbonsaeure-(10) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1,1']bicyclohexyl-1,1'-diene (1128-65-0) + 4-phenylcinnamic acid (88241-65-0,88241-67-2,13026-23-8) → 9--Δ4a-dodecahydro-phenanthren-carbonsaeure-(10) (97013-75-7)

Guidance literature:

With 2,4,6-Trinitrophenol; hydroquinone; at 180 - 200 ℃;

Reference yield:

9--Δ4a-dodecahydro-phenanthren-carbonsaeure-(10) (97013-75-7) → 2-Phenyl-5,6,7,8-dicyclohexano-fluoren (103652-47-7)

Guidance literature:

With phosphorus pentoxide; at 320 - 340 ℃;

Reference yield:

9--Δ4a-dodecahydro-phenanthren-carbonsaeure-(10) (97013-75-7) → 9-(4-biphenyl)phenanthrene (95950-75-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 300 °C

2: Se / 340 - 350 °C

With selenium;

upstream raw materials:

[1,1']bicyclohexyl-1,1'-diene

4-phenylcinnamic acid

Downstream raw materials:

2-Phenyl-5,6,7,8-dicyclohexano-fluoren

9-(4-biphenyl)phenanthrene

2-Phenyl-5,6,7,8-dibenzo-fluoren

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