Technology Process of C15H14N2O6
There total 9 articles about C15H14N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; potassium carbonate;
In
N,N-dimethyl-formamide;
at 120 ℃;
for 4h;
DOI:10.2174/1570180811310040011
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / water / 2 h / Reflux
2: potassium carbonate; copper(l) iodide / N,N-dimethyl-formamide / 4 h / 120 °C
With
hydrogenchloride; copper(l) iodide; potassium carbonate;
In
water; N,N-dimethyl-formamide;
2: |Ullmann Condensation;
DOI:10.2174/1570180811310040011
- Guidance literature:
-
Multi-step reaction with 6 steps
1: nitric acid; sulfuric acid / 2 h / 70 °C
2: potassium carbonate; potassium iodide / acetone / Reflux
3: potassium permanganate; water / 8 h / Reflux
4: palladium 10% on activated carbon / tetrahydrofuran / 24 h / 20 °C
5: sodium nitrite; hydrogenchloride; potassium iodide / dichloromethane / 4 h / 0 - 20 °C
6: potassium carbonate; copper(l) iodide / N,N-dimethyl-formamide / 4 h / 120 °C
With
hydrogenchloride; potassium permanganate; copper(l) iodide; sulfuric acid; palladium 10% on activated carbon; water; nitric acid; potassium carbonate; potassium iodide; sodium nitrite;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;
5: |Sandmeyer Reaction / 6: |Ullmann Condensation;
DOI:10.2174/1570180811310040011
