4-(trimethylstannyl)cyclohexyl trimethylsilyl ether

Base Information

Chemical Name:4-(trimethylstannyl)cyclohexyl trimethylsilyl ether
CAS No.:130451-26-2
Molecular Formula:C₁₂H₂₈OSiSn
Molecular Weight:335.149
Hs Code.:

Synonyms:

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Chemical Property of 4-(trimethylstannyl)cyclohexyl trimethylsilyl ether

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Technology Process of 4-(trimethylstannyl)cyclohexyl trimethylsilyl ether

There total 1 articles about 4-(trimethylstannyl)cyclohexyl trimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1066-45-1
trimethyltin(IV)chloride

: 146819-99-0
trans-1-iodo-4-(trimethylsiloxy)cyclohexane

: 130451-26-2,146820-00-0,130451-25-1
4-(trimethylstannyl)cyclohexyl trimethylsilyl ether

Guidance literature:: With lithium; In tetrahydrofuran; addn. of a THF soln. of Me3SnCl to cut Li wire in THF with rapid stirring at 0°C; stirring for 24 h; addn. to a soln. of 4-iodocyclohexyl trimethylsilyl ether in THF; stirring at room temp. for 2 days;; removal of solvent; extn. with hexane; removal of hexane and distn. at rudeced pressure; cis/trans mixt. obtained;;

Reference yield:

: 130451-26-2,146820-00-0,130451-25-1
4-(trimethylstannyl)cyclohexyl trimethylsilyl ether

: 106993-04-8,106993-03-7,150857-88-8
cis-4-trimethylstannylcyclohexan-1-ol

: 106993-04-8,106993-03-7,150857-88-8
trans-4-trimethylstannylcyclohexan-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; addn. of a THF soln. of (C4H9)4NF to a soln. of (CH3)3SnC6H10OSi(CH3)3 in THF; stirring for 24 h at room temp.;; removal of solvent; addn. of hexane; filtration; evapn. of the filtrate; sublimation at 40°C and 0.1 mmHg; chromy. (Al2O3, hexane, hexane/CCl4 (1:1), CCl4, CCl4/ether (1:1), ether, ether/CHCl3 (1:1) and then CHCl3; elem. anal.;;