Technology Process of 3-methylene-7-benzylidenebicyclo<3.3.1>nonane
There total 5 articles about 3-methylene-7-benzylidenebicyclo<3.3.1>nonane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
zinc copper;
In
N,N-dimethyl-formamide;
1. stirring 30 min ; 2. reflux 1.5 min;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: SOCl2
2: 1. CdCl2 / 1. (C2H5)2O, stirring 1 h, reflux 1 h; 2. C6H6 reflux 3 h
3: 98 percent / LiAlH4 / diethyl ether
4: 90 percent / 63percent aq HBr / 15 h / Heating
5: 78 percent Chromat. / zinc-copper couple / dimethylformamide / 1. stirring 30 min ; 2. reflux 1.5 min
With
lithium aluminium tetrahydride; thionyl chloride; zinc copper; hydrogen bromide; cadmium(II) chloride;
In
diethyl ether; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1. CdCl2 / 1. (C2H5)2O, stirring 1 h, reflux 1 h; 2. C6H6 reflux 3 h
2: 98 percent / LiAlH4 / diethyl ether
3: 90 percent / 63percent aq HBr / 15 h / Heating
4: 78 percent Chromat. / zinc-copper couple / dimethylformamide / 1. stirring 30 min ; 2. reflux 1.5 min
With
lithium aluminium tetrahydride; zinc copper; hydrogen bromide; cadmium(II) chloride;
In
diethyl ether; N,N-dimethyl-formamide;
