(3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone

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Chemical Name:(3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone
CAS No.:191722-63-1
Molecular Formula:C₂₅H₃₆N₁₀O₈
Molecular Weight:604.623
Hs Code.:

(3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone

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Chemical Property of (3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone

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Technology Process of (3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone

There total 1 articles about (3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: [(3S,9S,12S,15S)-15-Amino-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-2,5,8,11,14-pentaoxo-1,4,7,10,13-pentaaza-cyclohexadec-(6Z)-ylidenemethyl]-urea

: 191722-63-1
(3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone

Guidance literature:: In 1,4-dioxane; water;
DOI:10.1016/S0960-894X(97)00188-1

Reference yield:

: 191722-63-1
(3S,9S,12S,15S)-15-Amino-6-[1-benzyloxyamino-meth-(Z)-ylidene]-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-1,4,7,10,13-pentaaza-cyclohexadecane-2,5,8,11,14-pentaone

: 1-[(3S,9S,12S,15S)-6-Aminomethyl-9,12-bis-hydroxymethyl-3-((R)-2-imino-hexahydro-pyrimidin-4-yl)-2,5,8,11,14-pentaoxo-1,4,7,10,13-pentaaza-cyclohexadec-15-yl]-3-(4-cyclohexyl-phenyl)-urea

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / Ambient temperature

2: TFA, Et₃SiH

3: H₂ / Pd black / methanol

With triethylsilane; hydrogen; trifluoroacetic acid; palladium; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)00188-1