CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4

Base Information

Chemical Name:CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4
CAS No.:131629-82-8
Molecular Formula:C₂₄H₂₀B*C₄₀H₆₁CoO₈P₄
Molecular Weight:1172.04
Hs Code.:

CoH(P(OC<sub>2</sub>H<sub>5</sub>)2(C<sub>6</sub>H<sub>5</sub>))4<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=CoH(P(OC<sub>2</sub>H<sub>5</sub>)2(C<sub>6</sub>H<sub>5</sub>))4B(C<sub>6</sub>H<sub>5</sub>)4

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Chemical Property of CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4

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Technology Process of CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4

There total 2 articles about CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 41089-88-7,33516-93-7
hydrido(phosphonite)cobalt(I)

: 459-44-9
4-methylbenzenediazonium tetrafluoroborate

: 131629-82-8
CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4

Guidance literature:: With NaB(C₆H₅)4; In dichloromethane; cooling of a soln. of Co-compd. to -80°C (under Ar, Schlenk app.)and quick addn. to diazonium compd. at the same temp., warming to room temp. in 20 min, shaking for 30-40 min; solvent removal under reduced pressure, then triturating in EtOH, addn. of NaBPH4, crystn. from CH2Cl2/EtOH, elem. anal.;
DOI:10.1039/DT9900002979

Reference yield:

: 41089-88-7,33516-93-7
hydrido(phosphonite)cobalt(I)

: 143-66-8
sodium tetraphenyl borate

: 131629-82-8
CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4

Guidance literature:: In acetonitrile; Electrolysis; inert atmosphere, electrolysis of the Co complex at -0.2 V versus SCE in CH3CN containing NaClO4 as supporting electrolyte, Pt and glassy-C electrodes, evapn. to dryness, extn. (CH2Cl2), evapn., oil treated with ethanol, addn. of NaBPh4, pptn.; filtration, crystn. (CH2Cl2 and ethanol), elem. anal.;
DOI:10.1039/DT9940000695

Reference yield: 80.0%

: 131629-82-8
CoH(P(OC₂H₅)2(C₆H₅))4⁽¹⁺⁾*B(C₆H₅)4^(1-)=CoH(P(OC₂H₅)2(C₆H₅))4B(C₆H₅)4

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 131682-50-3
Co((CH₃)2C₆H₃NC)3(P(OC₂H₅)2C₆H₅)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co((CH₃)2C₆H₃NC)3(P(OC₂H₅)2C₆H₅)2B(C₆H₅)4

Guidance literature:: In dichloromethane; addn. of an excess of isocyanide to soln. of Co-compd. (under Ar, Schlenk app.), stirring for 30 min; solvent removal under reduced pressure, treating of residue with EtOH, crystn. from EtOH/CH2Cl2, elem. anal.;
DOI:10.1039/DT9900002979