3-Aminomethyl-5-trifluoromethyl-benzylamine

Base Information

Chemical Name:3-Aminomethyl-5-trifluoromethyl-benzylamine
CAS No.:214400-69-8
Molecular Formula:C₉H₁₁F₃N₂
Molecular Weight:204.195
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Aminomethyl-5-trifluoromethyl-benzylamine

Chemical Property:

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Technology Process of 3-Aminomethyl-5-trifluoromethyl-benzylamine

There total 4 articles about 3-Aminomethyl-5-trifluoromethyl-benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 214400-68-7
5-Trifluoromethyl-isophthalonitrile

: 214400-69-8
3-Aminomethyl-5-trifluoromethyl-benzylamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 2h; Yield given; Ambient temperature;
DOI:10.1021/jo980441p

Reference yield:

: 455-14-1
4-trifluoromethylphenylamine

: 214400-69-8
3-Aminomethyl-5-trifluoromethyl-benzylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / ICl / acetic acid; H₂O / 1 h / 80 °C

2: NaNO₂, H₂SO₄, H₃PO₂ / H₂O / 7 h / -10 °C

3: 61 percent / hexamethylphosphoric acid triamide / 5 h / 90 °C

4: LiAlH₄ / diethyl ether / 2 h / Ambient temperature

With lithium aluminium tetrahydride; sulfuric acid; hypophosphorous acid; Iodine monochloride; sodium nitrite; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; water; acetic acid;
DOI:10.1021/jo980441p

Reference yield:

: 214400-67-6
1,3-Diiodo-5-trifluoromethyl-benzene

: 214400-69-8
3-Aminomethyl-5-trifluoromethyl-benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / hexamethylphosphoric acid triamide / 5 h / 90 °C

2: LiAlH₄ / diethyl ether / 2 h / Ambient temperature

With lithium aluminium tetrahydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1021/jo980441p