(Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2

Base Information

Chemical Name:(Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2
CAS No.:289487-35-0
Molecular Formula:C₄₅H₅₃Cl₃Ir₂P₂
Molecular Weight:1146.66
Hs Code.:

Synonyms:

Suppliers and Price of (Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2

There total 1 articles about (Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 12354-84-6,12354-85-7
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

: ((C5(CH3)5)IrCl)2(μ-H)2

: 2071-20-7
bis-diphenylphosphinomethane

: 289487-35-0
(Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2

Guidance literature:: In tetrahydrofuran; under Ar; adding THF to mixt. of Ir complex and dppm, stirring at room temp. for 20.5 h, adding ((C5Me5)IrCl2)2, stirring at room temp. for 30 min; filtration of ppt., washing with Et2O, drying; elem. anal.;
DOI:10.1039/b001239o

Reference yield: 79.0%

: 289487-35-0
(Cl)(hydrido)(pentamethylcyclopentadienyl)Ir(μ-bis(diphenylphosphino)methane)Ir(pentamethylcyclopentadienyl)Cl2

: 2923-28-6
silver trifluoromethanesulfonate

: [(pentamethylcyclopentadienyliridium)2(μ-bis(diphenylphosphino)methane)(μ-hydrido)(μ-Cl)][trifluoromethanesulfonate]2

Guidance literature:: In tetrahydrofuran; under Ar; adding THF to mixt. of Ir complex and AgOTf, stirring at roomtemp. for 35 min; evapn., chromy. (silica gel, MeOH), evapn.; elem. anal.;
DOI:10.1039/b001239o