13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Base Information

Chemical Name:13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene
CAS No.:84735-05-7
Molecular Formula:C₂₅H₁₇N₃O₄
Molecular Weight:423.428
Hs Code.:

13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzo<de>naphthacene

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Chemical Property of 13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

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Technology Process of 13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

There total 5 articles about 13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 108-24-7
acetic anhydride

: 84735-01-3
4-Amino-5-imino-12-methoxy-9-methyl-11-oxo-2-phenyl-5H,11H-pyrano<3',2':6,7><1>benzopyrano<3,4-c>pyridine

: 84735-05-7
13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Guidance literature:: With pyridine; for 1h; boiling water bath;
DOI:10.1055/s-1982-30074

Reference yield:

: 5769-02-8
2-methyl-2-phenyl[1,3]dithiolane

: 84735-05-7
13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Guidance literature:: Multi-step reaction with 3 steps

2: 65 percent / ammonium acetate / ethanol / 1 h / Heating

3: 55 percent / pyridine / 1 h / boiling water bath

With pyridine; ammonium acetate; In ethanol;
DOI:10.1055/s-1982-30074

Reference yield:

: 7338-51-4
7-hydroxy-5-methoxy-2-methyl-4-oxo-4H-chromene-6-carbaldehyde

: 84735-05-7
13-Methoxy-5,10-dimethyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / ammonium acetate / ethanol / 1 h

2: 65 percent / ammonium acetate / ethanol / 1 h / Heating

3: 55 percent / pyridine / 1 h / boiling water bath

With pyridine; ammonium acetate; In ethanol;
DOI:10.1055/s-1982-30074