2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester

Base Information

Chemical Name:2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester
CAS No.:433922-97-5
Molecular Formula:C₇₀H₈₅N₅O₁₂S
Molecular Weight:1220.54
Hs Code.:

2-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-<i>N</i>-trityl-succinamic acid 1-{[<i>tert</i>-butoxycarbonyl-(2-<i>tert</i>-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester

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Chemical Property of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester

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Technology Process of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester

There total 8 articles about 2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 132388-59-1
L-Asn(Trt)

: 433922-96-4
3-{tert-butoxycarbonyl-[2-hydroxy-5-methyl-3-(2,4,6-trimethyl-benzenesulfonylamino)-hexyl]-amino}-N-isopropyl-succinamic acid tert-butyl ester

: 433922-97-5
2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide;

Reference yield:

: 3-amino-N-isopropyl-succinamic acid tert-butyl ester

: 433922-97-5
2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / DIPEA / propan-2-ol

2: 95 percent / Et₃N

3: 61 percent / DCC; DMAP

With dmap; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In isopropyl alcohol;

Reference yield:

: 433922-92-0
2,4,6-Trimethyl-N-((R)-3-methyl-1-(R)-oxiranyl-butyl)-benzenesulfonamide

: 433922-97-5
2-(9H-fluoren-9-ylmethoxycarbonylamino)-N-trityl-succinamic acid 1-{[tert-butoxycarbonyl-(2-tert-butoxycarbonyl-1-isopropylcarbamoyl-ethyl)-amino]-methyl}-4-methyl-2-(2,4,6-trimethyl-benzenesulfonylamino)-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / DIPEA / propan-2-ol

2: 95 percent / Et₃N

3: 61 percent / DCC; DMAP

With dmap; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In isopropyl alcohol;