1-phenylcyclobutylmethyl chloride

Base Information

Chemical Name:1-phenylcyclobutylmethyl chloride
CAS No.:149050-19-1
Molecular Formula:C₁₁H₁₃Cl
Molecular Weight:180.677
Hs Code.:

Synonyms:

Suppliers and Price of 1-phenylcyclobutylmethyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenylcyclobutylmethyl chloride

Chemical Property:

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Technology Process of 1-phenylcyclobutylmethyl chloride

There total 4 articles about 1-phenylcyclobutylmethyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 70775-57-4
(1-phenylcyclobutyl)methanol

: 149050-19-1
1-phenylcyclobutylmethyl chloride

Guidance literature:: With tetrachloromethane; triphenylphosphine; for 48h; Ambient temperature;
DOI:10.1016/0022-328X(93)80060-O

Reference yield:

: 14377-68-5
1-phenylcyclobutanecarbonitrile

: 149050-19-1
1-phenylcyclobutylmethyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / KOH / bis-(2-hydroxy-ethyl) ether

2: 87 percent / LiAlH₄ / diethyl ether

3: 50 percent / CCl₄, Ph₃P / 48 h / Ambient temperature

With tetrachloromethane; potassium hydroxide; lithium aluminium tetrahydride; triphenylphosphine; In diethyl ether; diethylene glycol;
DOI:10.1016/0022-328X(93)80060-O

Reference yield:

: 37828-19-6
1-(phenyl)cyclobutane-1-carboxylic acid

: 149050-19-1
1-phenylcyclobutylmethyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / LiAlH₄ / diethyl ether

2: 50 percent / CCl₄, Ph₃P / 48 h / Ambient temperature

With tetrachloromethane; lithium aluminium tetrahydride; triphenylphosphine; In diethyl ether;
DOI:10.1016/0022-328X(93)80060-O