Technology Process of rac-Hydnocarpin-5',7',4''-trimethylether
There total 9 articles about rac-Hydnocarpin-5',7',4''-trimethylether which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
selenium(IV) oxide;
In
pentan-1-ol;
for 15h;
Heating;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 26 percent / piperidine / ethanol / 14 h / Heating
2: 1) 10percent HCl; 2) NaOAc / 1) methanol, reflux, 30 min.; 2) water, reflux, 4 h
3: 98 percent / pyridine / Ambient temperature
4: NBS, benzoylperoxide / CCl4 / 0.33 h / Heating
5: 1) 1N NaOCH3 2.) K2CO3 / 1) room temperature, 12 h, MeOH 2) reflux, 3 h, acetone
With
piperidine; hydrogenchloride; N-Bromosuccinimide; Perbenzoic acid; sodium methylate; sodium acetate; potassium carbonate;
In
pyridine; tetrachloromethane; ethanol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 35 percent / K2CO3 / acetone / Heating
2: 72 percent / OsO4, NaIO4 / dioxane / 12 h / Ambient temperature
3: 26 percent / piperidine / ethanol / 14 h / Heating
4: 1) 10percent HCl; 2) NaOAc / 1) methanol, reflux, 30 min.; 2) water, reflux, 4 h
5: 98 percent / pyridine / Ambient temperature
6: NBS, benzoylperoxide / CCl4 / 0.33 h / Heating
7: 1) 1N NaOCH3 2.) K2CO3 / 1) room temperature, 12 h, MeOH 2) reflux, 3 h, acetone
With
piperidine; hydrogenchloride; sodium periodate; N-Bromosuccinimide; osmium(VIII) oxide; Perbenzoic acid; sodium methylate; sodium acetate; potassium carbonate;
In
1,4-dioxane; pyridine; tetrachloromethane; ethanol; acetone;
![(E)-3-[(2S,3S)-2-(3,4-Dimethoxy-phenyl)-3-hydroxymethyl-2,3-dihydro-benzo[1,4]dioxin-6-yl]-1-(2-hydroxy-4,6-dimethoxy-phenyl)-propenone](/Databaselist/images/loading.webp)
