5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate

Base Information

Chemical Name:5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate
CAS No.:140660-55-5
Molecular Formula:C₃₃H₄₂N₄O₇
Molecular Weight:606.719
Hs Code.:

5-<3-<2-<N-(benzyloxycarbonyl)amino>ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate

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Chemical Property of 5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate

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Technology Process of 5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate

There total 4 articles about 5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153-98-0,21591-86-6
serotonin hydrochloride

: 140660-55-5
5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 67.7 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

2: 1.) BOP-Cl, DMAP, TEA / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, RT, 24 h

With pyridine; dmap; TEA; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; In dichloromethane;
DOI:10.1021/jm00089a015

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 140660-55-5
5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 67.7 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

2: 1.) BOP-Cl, DMAP, TEA / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, RT, 24 h

With pyridine; dmap; TEA; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; In dichloromethane;
DOI:10.1021/jm00089a015

Reference yield:

: 88321-09-9
aloxistatin

: 140660-55-5
5-<3-<2-ethyl>-1H-indolyl> (+)-(2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / 5 h / 0 - 20 °C

2: 1.) BOP-Cl, DMAP, TEA / 1.) CH₂Cl₂, 0 deg C, 20 min, 2.) CH₂Cl₂, RT, 24 h

With dmap; potassium hydroxide; TEA; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; In ethanol;
DOI:10.1021/jm00089a015