10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid

Base Information

Chemical Name:10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid
CAS No.:163041-00-7
Molecular Formula:C₇₃H₉₁NO₁₂
Molecular Weight:1174.53
Hs Code.:

10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid

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Chemical Property of 10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid

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Technology Process of 10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid

There total 3 articles about 10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1054656-80-2
N-[(2S,3S,4S,5R)-4-Benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-2-(10-oxo-decyl)-tetrahydro-pyran-3-yl]-acetamide

: 163041-00-7
10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; In tert-butyl alcohol; for 0.166667h; Yield given; Ambient temperature;
DOI:10.1021/jo00112a040

Reference yield:

: 1053623-77-0
N-[(2S,3S,4S,5R)-4-Benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-2-(10-hydroxy-decyl)-tetrahydro-pyran-3-yl]-acetamide

: 163041-00-7
10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: (PPh₃)3RuCl₂, 3 Angstroem molecular sieves / benzene / 1 h / Ambient temperature

2: 10percent aq. NaClO₂, 10percent aq. NaH₂PO₄*H₂O / 2-methyl-propan-2-ol; various solvent(s) / 0.17 h / Ambient temperature

With sodium chlorite; sodium dihydrogenphosphate; tris(triphenylphosphine)ruthenium(II) chloride; 3 A molecular sieve; In tert-butyl alcohol; benzene;
DOI:10.1021/jo00112a040

Reference yield:

: 1053616-32-2
C₈₁H₁₀₁NO₁₂

: 163041-00-7
10-{(2S,3S,4S,5R)-3-Acetylamino-4-benzyloxy-5-[(2S,3S,5R,6R)-5-benzyloxy-6-benzyloxymethyl-3-((2S,3R,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-ylmethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-decanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: DDQ, phosphate buffer (pH 7) / CH₂Cl₂ / 1 h / 0 °C

2: (PPh₃)3RuCl₂, 3 Angstroem molecular sieves / benzene / 1 h / Ambient temperature

3: 10percent aq. NaClO₂, 10percent aq. NaH₂PO₄*H₂O / 2-methyl-propan-2-ol; various solvent(s) / 0.17 h / Ambient temperature

With sodium chlorite; sodium dihydrogenphosphate; tris(triphenylphosphine)ruthenium(II) chloride; phosphate buffer; 3 A molecular sieve; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; tert-butyl alcohol; benzene;
DOI:10.1021/jo00112a040