dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate

Base Information

• Chemical Name: dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate
• CAS No.: 123948-61-8
• Molecular Formula: C₃₃H₅₀N₃O₈P
• Molecular Weight: 647.749
• Mol file: 123948-61-8.mol

Synonyms:

Chemical Property of dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate

There total 4 articles about dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

dodecyl N-<4-<4-(5-hydroxypentyloxy)phenylazo>benzoyl>-L-alaninate (135424-90-7) + trichlorophosphate (10025-87-3,12599-09-6,63736-95-8,39380-77-3) → dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate (123948-61-8)

Guidance literature:

In tetrahydrofuran; for 12h; Ambient temperature;

Reference yield:

5-bromopentan-1-ol (34626-51-2) → dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate (123948-61-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 57 percent / KOH / ethanol / 24 h / Heating

2: 40 percent / triethylamine, diethyl cyanophosphate / tetrahydrofuran / 48 h / Ambient temperature

3: 32 percent / tetrahydrofuran / 12 h / Ambient temperature

With potassium hydroxide; diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; ethanol;

Reference yield:

4-<4-(5-hydroxypentyloxy)phenylazo>benzoic acid (135424-89-4) → dodecyl N<4-<4-(5-phosphopentyloxy)phenylazo>benzoyl>-L-alaninate (123948-61-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / triethylamine, diethyl cyanophosphate / tetrahydrofuran / 48 h / Ambient temperature

2: 32 percent / tetrahydrofuran / 12 h / Ambient temperature

With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran;

upstream raw materials:

dodecyl N-<4-<4-(5-hydroxypentyloxy)phenylazo>benzoyl>-L-alaninate

trichlorophosphate

5-bromopentan-1-ol

4-<4-(5-hydroxypentyloxy)phenylazo>benzoic acid

Refernces