(η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate)

Base Information

Chemical Name:(η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate)
CAS No.:103473-75-2
Molecular Formula:BF₄*C₄₂H₃₅FeO₇P₂
Molecular Weight:856.335
Hs Code.:

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Chemical Property of (η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate)

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Technology Process of (η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate)

There total 3 articles about (η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 101-02-0
triphenyl phosphite

: {C₅H₅Fe(CO)(S(CH₃)2)2}⁽¹⁺⁾*BF₄^(1-)={C₅H₅Fe(CO)(S(CH₃)2)2}BF₄

: 103473-75-2
(η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate)

Guidance literature:: In 1,2-dichloro-ethane; byproducts: (CH3)2S; Ar-atmosphere; refluxing (15 min);; filtration, evapn. (vac.), stirring with petroleum ether/Et2O (1:1), drying (vac.); elem. anal.;;
DOI:10.1016/0022-328X(85)80248-5

Reference yield: 45.0%

: 101-02-0
triphenyl phosphite

: 52326-25-7
(η5-Cp)(CO)Fe(η3-allyl)

: 103473-75-2
(η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate)

Guidance literature:: In dichloromethane; Treating a soln. of (C5H5)(CO)Fe(η3-C3H5) at -78°C with P(OPh)3 followed by warming to room temp. and refluxing for 10 h, addn. of the resulting green soln. to Et2O at -78°C.; Warming to room temp., removing solvent by a double-ended needle, drying under vac.;