(η5-Cp)(CO)Fe(η3-allyl)

Base Information

Chemical Name:(η5-Cp)(CO)Fe(η3-allyl)
CAS No.:52326-25-7
Molecular Formula:C₉H₁₀FeO
Molecular Weight:190.025
Hs Code.:

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Chemical Property of (η5-Cp)(CO)Fe(η3-allyl)

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Technology Process of (η5-Cp)(CO)Fe(η3-allyl)

There total 1 articles about (η5-Cp)(CO)Fe(η3-allyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38960-10-0
allyl(cyclopentadienyl)iron(II) dicarbonyl

: [Fe2(η-C5H5)2(CO)(PPh3)(μ-CO)2]

: 52326-25-7
(η5-Cp)(CO)Fe(η3-allyl)

Guidance literature:: In benzene; byproducts: CO; Irradiation (UV/VIS); under Ar, irradn. of benzene soln. of Fe complex in presence of PPh3 and trace of (CpFe(CO)2)2; not isolated, detected by NMR;

Reference yield: 87.0%

: tetrafluoroboric acid

: 52326-25-7
(η5-Cp)(CO)Fe(η3-allyl)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 35004-56-9
(η5-Cp)(CO)Fe(Ph2PCH2CH2PPh2)(tetrafluoroborate)

Guidance literature:: In diethyl ether; dichloromethane; Treating a CH2Cl2 soln. at -78°C of (C5H5)(CO)Fe(η3-C3H5) with HBF4-ether soln., reacting the resulting dark green soln. with Ph2PCH2CH2PPh2 followed by warming the soln. to room temp.; Pptg. with ether, centrifuging and drying under vac.;

Reference yield: 45.0%

: 101-02-0
triphenyl phosphite

: 52326-25-7
(η5-Cp)(CO)Fe(η3-allyl)

: 103473-75-2
(η5-Cp)(CO)Fe(triphenyl phosphite)2(hexafluoroborate)

Guidance literature:: In dichloromethane; Treating a soln. of (C5H5)(CO)Fe(η3-C3H5) at -78°C with P(OPh)3 followed by warming to room temp. and refluxing for 10 h, addn. of the resulting green soln. to Et2O at -78°C.; Warming to room temp., removing solvent by a double-ended needle, drying under vac.;