4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide

Base Information

• Chemical Name: 4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide
• CAS No.: 182694-58-2
• Molecular Formula: C₁₂H₈F₈INO₅S₂
• Molecular Weight: 589.223
• Mol file: 182694-58-2.mol

Synonyms:

Chemical Property of 4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide

There total 1 articles about 4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

styrene oxide (96-09-3) + ICF2CF2OCF2CF2SO2N=S=O (135705-81-6) → 1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodoethoxy)-ethanesulfonyl amide (148716-83-0) + 4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide (182694-58-2)

Guidance literature:

In benzene; for 4h; Ambient temperature;

DOI:10.1016/0022-1139(96)03467-7

Reference yield: 91.0%

4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide (182694-58-2) → 1,1,2,2-Tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonic acid (2-hydroxy-1-phenyl-ethyl)-amide

Guidance literature:

With hydrogenchloride; for 2h; Ambient temperature;

DOI:10.1016/0022-1139(96)03467-7

Reference yield: 58.0%

4-Phenyl-3-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-[1,2,3]oxathiazolidine 2-oxide (182694-58-2) → 2-Phenyl-1-[1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoro-2-iodo-ethoxy)-ethanesulfonyl]-aziridine

Guidance literature:

at 160 ℃;

DOI:10.1016/0022-1139(96)03467-7

upstream raw materials:

styrene oxide

ICF₂CF₂OCF₂CF₂SO₂N=S=O