C₄₇H₈₃BO₄Si₂

Base Information

Chemical Name:C₄₇H₈₃BO₄Si₂
CAS No.:185409-77-2
Molecular Formula:C₄₇H₈₃BO₄Si₂
Molecular Weight:779.156
Hs Code.:

C<sub>47</sub>H<sub>83</sub>BO<sub>4</sub>Si<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₈₃BO₄Si₂

Chemical Property:

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Technology Process of C₄₇H₈₃BO₄Si₂

There total 8 articles about C₄₇H₈₃BO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85116-37-6
(-)-diisopinocamphenylborane chloride

: 185409-75-0
(4S,6S)-8-benzyloxy-4-(tert-butyldimethylsiloxy)-6-(triethylsiloxy)-2-octanone

: 185409-77-2
C₄₇H₈₃BO₄Si₂

Guidance literature:: With triethylamine; In diethyl ether; at 0 ℃; for 0.666667h;
DOI:10.1039/b504146e

Reference yield:

: 1-(benzyloxy)hex-5-en-3-one

: 185409-77-2
C₄₇H₈₃BO₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 3.64 g / aq. NaOH; H₂O₂ / diethyl ether / 16 h / Heating

2.1: 98 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -78 °C

3.1: NaHCO₃; O₃ / CH₂Cl₂ / -78 °C

3.2: 95 percent / PPh₃ / CH₂Cl₂ / 3.5 h / 20 °C

4.1: diethyl ether / 20 h / -78 - -20 °C

4.2: aq. H₂O₂ / methanol / 1 h / 20 °C

5.1: 97 percent / imidazole / dimethylformamide / 16 h / 20 °C

6.1: Et₃N / diethyl ether / 0.67 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; sodium hydroxide; dihydrogen peroxide; sodium hydrogencarbonate; ozone; triethylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b504146e

Reference yield:

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 185409-77-2
C₄₇H₈₃BO₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 98 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -78 °C

2.1: NaHCO₃; O₃ / CH₂Cl₂ / -78 °C

2.2: 95 percent / PPh₃ / CH₂Cl₂ / 3.5 h / 20 °C

3.1: diethyl ether / 20 h / -78 - -20 °C

3.2: aq. H₂O₂ / methanol / 1 h / 20 °C

4.1: 97 percent / imidazole / dimethylformamide / 16 h / 20 °C

5.1: Et₃N / diethyl ether / 0.67 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; sodium hydrogencarbonate; ozone; triethylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b504146e