Technology Process of C54H70O6S
There total 6 articles about C54H70O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine;
In
benzene-d6;
for 21h;
Ambient temperature;
DOI:10.1021/jo970287r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 53 percent / Triton B-TBHP
2: 1.) LAH, 2.) Jones reagent / 1.) Et2O, reflux
3: 62 percent / tetrahydrofuran / 0.75 h / -60 °C
4: 33 percent / 2,6-lutidine / benzene-d6 / 21 h / Ambient temperature
With
2,6-dimethylpyridine; tert.-butylhydroperoxide; lithium aluminium tetrahydride; jones reagent; N-benzyl-trimethylammonium hydroxide;
In
tetrahydrofuran; benzene-d6;
DOI:10.1021/jo970287r
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 92 percent / CuBr2
2: 71 percent / CaCO3 / dimethylformamide / 0.5 h / Heating
3: 53 percent / Triton B-TBHP
4: 1.) LAH, 2.) Jones reagent / 1.) Et2O, reflux
5: 62 percent / tetrahydrofuran / 0.75 h / -60 °C
6: 33 percent / 2,6-lutidine / benzene-d6 / 21 h / Ambient temperature
With
2,6-dimethylpyridine; tert.-butylhydroperoxide; lithium aluminium tetrahydride; jones reagent; N-benzyl-trimethylammonium hydroxide; calcium carbonate; copper(ll) bromide;
In
tetrahydrofuran; benzene-d6; N,N-dimethyl-formamide;
DOI:10.1021/jo970287r